1,4-Bis[(1H-pyrazol-1-yl)meth­yl]benzene dihydrate

نویسندگان

  • Ai-E Shi
  • Yan-Jun Hou
  • Yi-Ming Zhang
  • Guang-Feng Hou
  • Jin-Sheng Gao
چکیده

The asymmetric unit of the title compound, C(14)H(14)N(4)·2H(2)O consists of two half-mol-ecules of the main mol-ecule, each situated on an inversion center, and two mol-ecules of water. One-dimensional chains of water mol-ecules are built up by O-H⋯O hydrogen bonds which are then linked with the main mol-ecule via O-H⋯N hydrogen bonds, forming a two-dimensional supra-molecular network in the ac plane.

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The title zinc complex, [ZnCl(2)(C(18)H(22)N(4))], contains a bidentate 1,2-bis(3,5-dimethyl-1H-pyrazol-1-ylmeth-yl)benz-ene ligand that binds to the zinc atom, forming a nine-membered metallocyclic ring. The geometry about the Zn atom is distorted tetra-hedral, with the largest deviation observed in the magnitude of the Cl-Zn-Cl angle. Similar distortions are observed in the cobalt analogue an...

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عنوان ژورنال:

دوره 65  شماره 

صفحات  -

تاریخ انتشار 2009